Sampling and Sample Preparation in Field and Laboratory: Fundamentals and New Directions in Sample Preparation

Front Cover
Janusz Pawliszyn
Elsevier, Sep 9, 2002 - Science - 1131 pages
This title is the first comprehensive book on sampling and modern sample preparation techniques and has several main objectives: to facilitate recognition of sample preparation as both an integral part of the analytical process; to present a fundamental basis and unified theoretical approach for the professional development of sample preparation; to emphasize new developments in sample preparation technology; and to highlight the future impact of sample preparation on new directions in analytical science, particularly automation, miniaturization and field implementation.

Until recently, there has been relatively little scientific interest in sampling and sample preparation, however this situation is presently changing as sampling and sample preparation become integral parts of the analytical process with their own unique challenges and research opportunities.

Sampling and Sample Preparation for Field and Laboratory is an essential resource for all analytical chemists, and in particular those involved in method development. Not only does it cover the fundamental aspects of extraction, it also covers applications in various matrices and includes sampling strategies and equipment and how these can be integrated into the analytical process for maximum efficiency.
 

Contents

References
27
Sampling water and aqueous solutions
33
Sampling selected solid materials
61
Samplers for greasy doughy and fusible materials
67
45
69
6
78
1
87
6
94
Characterization of analyte binding and freely dissolved
241
4
250
Unified theory of extraction
253
Diffusionbased calibration
269
4
276
Liquidliquid extraction
297
Principles and practice of solidphase extraction
341
Solid phase microextraction
389

46
103
Sample Matrices
115
32
140
Automated measurement of atmospheric particle composition
161
3
175
200
216
Physicochemical properties of aqueous and solid environmental
219
Membrane extraction
479
Liquid membrane techniques
503
Membrane inlet mass spectrometry
531
Extraction techniques for solid samples
559
Hot subcritical water extraction
587
282
1046
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