Analysis of Carbohydrates by GLC and MSThis textbook is a comprehensive guide to analysis of carbohy-drates by gas-liquid chromatography and mass spectrometry. In addition to explaining the facets of carbohydrate analysis and their relation to each other, the text also contains in-depth reference in-formation useful to practitioners in the field. Improvements in car-bohydrate analyses methodology during the past six years are also highlighted. This extensively illustrated text provides excellent data for those in carbohydrate, agriculture, and food chemistry. |
Contents
Chapter | 1 |
Chapter | 12 |
HighPerformance Liquid Chromatography HPLC of Carbohydrates | 19 |
Chapter 4 | 35 |
Chapter 5 | 63 |
Preparation of Alditol Acetates and Their Analysis by Gas Chromatography GC | 87 |
Analysis of Monosaccharides as PerOAcetylated Aldononitrile PAAN Derivatives | 119 |
Chapter 8 | 135 |
Chapter 9 | 157 |
Sample Preparation | 217 |
Chapter 11 | 237 |
Miscellaneous Gas Chromatographic GC Analyses of Carbohydrates | 257 |
| 275 | |
Other editions - View all
Analysis of Carbohydrates by GLC and MS Christopher J. Biermann,Gary D. McGinnis Limited preview - 2021 |
Analysis of Carbohydrates by GLC and MS Christopher J. Biermann,Gary D. McGinnis Limited preview - 2021 |
Analysis of Carbohydrates by GLC and MS Christopher J. Biermann,Gary D. McGinnis No preview available - 2019 |
Common terms and phrases
acetic acid acetic anhydride acetylation acid hydrolysis aldononitrile acetates aldoses amino sugars Anal analysis of carbohydrates analyzed anomeric Biochem borohydride capillary column carboxyl catalyst cell walls cellulose CH2OH Chem Chromatogr cleavage components decomposition derivatization detection detector determination disaccharides DMSO eluting esters ethers evaporation FAB-MS Figure fragment ions fructose fucose galactose gas chromatography gas-liquid chromatography glucose glycoproteins glycosidic linkages hexitol HexNAc hexoses hydrolysis hydrolyzed hydroxyl groups internal standard ionization liquid chromatography mannose mass spectrometry methanide methanol methanolysis methoxylated carbons methyl glycosides mixture ml/min MO-TMS molecular ions monosaccharides muramic acid neutral and amino neutral sugars nitrogen O-alkyloximation O-methyloxime OAC HC oligosaccharides oxidation oximes partially methylated peaks permethylated polymers polysaccharides preparation procedure produced pyridine quantitative reaction reagent reducing residues rhamnose saccharides sample separation sialic acids silicone silylation sodium solution solvent spectra structure sulfate Sweeley temperature trifluoroacetic trimethylsilyl uronic acids volatile xylose