Pharmaceutical Drug AnalysisAbout the Book: During the past two decades, there have been magnificent and significant advances in both analytical instrumentation and computerized data handling devices across the globe. In this specific context the remarkable proliferation of windows |
Contents
PURITY AND MANAGEMENT | 3 |
THEORY AND TECHNIQUE OF QUANTITATIVE ANALYSIS | 41 |
ERRORS IN PHARMACEUTICAL ANALYSIS AND STATISTICAL | 71 |
3B Statistical Validation | 77 |
AQUEOUS TITRATIONS | 95 |
NONAQUEOUS TITRATIONS | 106 |
PERMANGANATE DICHROMATE AND CERIC SULPHATE | 125 |
IODIMETRIC AND IODOMETRIC TITRATIONS | 137 |
AMPEROMETRIC METHODS | 253 |
REFRACTOMETRY | 265 |
POLARIMETRY | 274 |
NEPHELOMETRY AND TURBIDIMETRY | 283 |
ULTRAVIOLET AND ABSORPTION METHODS | 293 |
INFRARED SPECTROPHOTOMETRY | 314 |
NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY | 339 |
EMISSION SPECTROSCOPY | 357 |
ARGENTOMETRIC METHODS | 151 |
COMPLEXOMETRIC ANALYSIS | 161 |
GRAVIMETRIC ANALYSIS | 173 |
THERMOANALYTICAL ANALYSIS | 193 |
DIAZOTIZATION SODIUM NITRITE TITRATION | 207 |
ESTIMATION OF PHENOLS AND RELATED COMPOUNDS | 213 |
KARL FISCHER METHOD FOR DETERMINATION OF WATER | 223 |
ELECTROCHEMICAL METHODS | 231 |
FLAME SPECTROSCOPY | 370 |
ATOMIC ABSORPTION SPECTROSCOPY | 378 |
ASSAY METHODS BASED ON SEPARATION TECHNIEQUES | 391 |
THIN LAYER CHROMATOGRAPHY TLC | 409 |
GAS LIQUID CHROMATOGRAPHY GLC | 431 |
HIGH PERFORMANCE LIQUID CHROMATOGRAPHY HPLC | 452 |
SIZE EXCLUSION CHROMATOGRAPHY | 476 |
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Common terms and phrases
absorbance absorption acetic acid AgNO3 ammonium amperometric amperometric titrations antibody atoms bromine burette Calcium Calculations chemical chloride chloroform chromatography Cognate Assays colour column complex components compounds concentration constant curve detector determination dilute disodium Dissolve drug electrode emission employed end-point equivalent errors ethanol extraction Figure filter flame frequency H₂O hapten HCIO Hence HPLC hydrochloric acid hydrochloride iodide iodine layer limit test liquid Materials Required measured metal minutes mixture ml DW ml of DW ml with DW mobile-phase molecule namely NaOH obtained optical oxidation perchloric acid pharmaceutical substances pipette potassium potassium bromate potassium iodide precipitate Procedure produce proton quantitative Radioimmunoassay reaction reagent refractive S.No sample sodium hydroxide sodium nitrite solubility solvent specific spectrophotometer spectroscopy spectrum standard solution sulphate technique temperature tetrabutylammonium hydroxide Theory titration method tube volume volumetric flask w/v soln wavelength Weigh accurately weight