USP 33 NF 28: United States Pharmacopeia [and] National Formulary. Reissue. Supplement 2.aUnited States Pharmacopeial Convention, 2010 - 491 pages |
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Acceptance criteria acetone ACS reagent grade ammonium Analysis Samples anhydrous assay blank calcium pantothenate Calculate the percentage chloride chloroform cholecalciferol Chromatography Chromatography 621 colorless column containing cool crystalline powder crystals cyanocobalamin detector dilute with water Dissolve ergocalciferol ethyl filter Freely soluble glycol hydrochloric acid hygroscopic Injection insoluble in ether labeled amount liquid magnesium methanol Method mg/mL mixture mL of water monograph NF category niacin niacinamide nitric acid nominal concentration peak area perchloric acid Ph.D Pharm.D Phosphate potassium practically insoluble Related Compound residue Sample solution µg/mL selenium slightly soluble sodium hydroxide solu soluble in alcohol soluble in chloroform soluble in methanol soluble in water solution and Sample solvent sparingly soluble Specific Standard solution Standard stock Standard stock solution Sulfate sulfuric acid System suitability thiamine tion titrate Transfer TS-Dissolve tubes USP Reference Standards vitamin volumetric flask water to volume weight White to off-white yellow